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55SiMnMo钢正火组织的精细结构和晶体学特征

罗承萍 , 刘正义 , 许麟康

材料研究学报

55SiMnMo 钢的正火组织由无碳化物上、下贝氏体,马氏体和残余奥氏体组成。贝氏体含有中脊线,组织单元和位错;马氏体含有孪晶;残余奥氏体含有高密度位错。奥氏体的位向关系和惯习面表明它以切变机制生成。从界面富碳和界面应力弛豫两方面阐述了贝氏体组织单元以及贝氏体片条的生成机制。

关键词: 贝氏体 , subunit , midrib , orientation relationship , habit plane

用相变晶体学指导Mg-Sn-Mn合金优化设计

石章智张文征

金属学报 doi:10.3724/SP.J.1037.2010.00323

以相变晶体学为主要原则对Mg-Sn-X合金进行优化设计. 在对现有镁合金系统充分调研的基础上, 根据Mg基体与析出相的相变晶体学匹配关系, 提出2条相变晶体学判据来判断可能沿Mg基体[0001]α方向择优生长的析出相. 根据这2条相变晶体学判据结合相图分析推测在Mg-Sn-Mn系统中可能得到沿Mg基体[0001]α方向择优生长的β-Mn析出相. 对Mg-7.5Sn-2.2Mn(质量分数, %)合金时效组织的TEM研究证实了上述判断. 研究结果表明, β-Mn析出相呈棒状, 长轴沿Mg基体[0001]α方向, 它与Mg基体的位向关系(OR)是: [0001]α///[211]β-Mn, [0110]α///[011]β-Mn, [2110]α//[111]β-Mn.

关键词: 镁合金设计 , crystallography of phase transformation , morphology of precipitates , orientation relationship

沉淀相变晶体学模型的研究进展

邱冬 , 张文征

金属学报

相变晶体学是对工程材料进行组织设计的重要理论基础。本文综述了国内外沉淀相变晶体学模型的最新研究进展,对各个模型的使用前提、适用条件、求解思路以及自身的局限性分别进行了评述;通过比较不同模型的在求解能力方面的差异,指出将O线模型和近重位位置模型相结合的方法将为理解相变晶体学特征提供更有力的理论工具。

关键词: 沉淀相变 , theoretical model , orientation relationship , habit plane , null

低碳钢中晶界铁素体/原奥氏体界面对贝氏体转变的影响

崔桂彬郭晖杨善武贺信莱

金属学报

采用电子背散射衍射 (EBSD) 研究了低碳Fe--C--Mn--Si钢中晶界铁素体/原奥氏体界面对贝氏体形核的影响. 通过两阶段等温热 处理, 获得了晶界铁素体和贝氏体的混合组织. 结合金相观察和取向测量, 发现晶界铁素体与贝氏铁素体之间的界面分为两种, 一种界面不清晰, 一种界面清晰. 分析表明, 在晶界铁素体/贝氏体界面不清晰一侧, 晶界铁素体与原奥氏体保持取向关系, 贝氏体在这类界面形 核生长, 且取向与晶界铁素体保持一致; 在晶界铁素体/贝氏体界面清晰一侧, 晶界铁素体与原奥氏体无取向关系, 且贝氏体与晶界铁素体之间取向差较大.

关键词: 低碳钢 , grain boundary ferrite , bainite , interface , nucleation , orientation relationship

MATRIX INVESTIGATION ON ISAICHEV ORIENTATION RELATIONSHIP

Z.Q. Sheng and H. Xiao(National Key Laboratory for Nuclear Fuel and Material , Nuclear Power Institute of China , Chengdu 610041 , China)Manuscript received in revised form 16 October 1998)

金属学报(英文版)

By means of TEM technique the orientation relationships of cementite, precipitated from islands of granular bainite during tempering, with ferrite have been objerved. By calculating the eigenvalue and eigenvector of transformation matrix, Isaichev relationship has been analyzed. The results indicate that Isaichev relationship indeed is the sum of Kungumov-Sachs relationship and Pitsch relationship, so the viempoint that the cementite with Isaichev relationship precipitates from austenite, instead of ferrite,is confirmed. Moreoven the matrix calculation shows that three reported orientation relationships among austenite, ferrite and cementite in pearlitic transformation cannot be simultaneously valid.

关键词: orientation relationship , null

原位生成Al2O3增强Al-4Mg基复合材料中的Al2O3/Al位向关系

欧阳柳章 , 罗承萍

金属学报

综合搅拌铸造法和原位反应制备了Al2O3颗粒增强Al-4Mg基复合材料,并对制备的Al-4Mg基复合材料进行了透射电镜(TEM)观察分析,发现Al2O3/Al之间不存在固定的位向关系。但存在如下优先的位向关系:( )Al2O3//(111) Al,[ ]Al2O3//[ ] Al,[ ]Al2O3//[ ] Al。

关键词: Al2O3/Al-4Mg复合材料 , orientation relationship , null

Cu-71.8%Ag共晶体中两相的台阶界面及晶体取向

刘嘉斌 , 曾跃武 , 孟亮

金属学报

采用熔铸法制备了Cu-71.8%Ag(质量分数)合金, 研究了共晶体中两相的位向关系和界面结构. 约50%的相界面两侧Cu和Ag两相位向对称于(111)晶面. 出现对称位向的相界面形态为台阶状, 台阶平面与(111)平行, 高度为(111)Cu和(111)Ag晶面间距的平均值, 宽度为3—4个(11-1)Cu晶面间距. 在此界面上, 每隔3—4个(11-1)Cu晶面间距出现一个点阵重合位置.

关键词: Cu-Ag合金 , orientation relationship , interfacial structur

FINE STRUCTURES OF BOTH INTERFACES AND INTERFACIAL REACTION PRODUCTS

LI Douxing PING Dehai NING Xiaoguang YE Hengqiang Laboratory of Atomic Imaging of Solids , Institute of Metal Research , Academia Sinica , Shenyang.China Professor , Institute of Metal Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The characteristic of interface depending on the atomic structure exerts an inportant,and sometime controlling,influence on performance of the interacial materials. The present paper reviews the main studies on fine structure of both the materials inter- faces and interfacial reaction products in semiconductor uperlattice,metal multilayer ceram- ics and composite materials by mean of selected area electron doffraction patterns and high resolution electron microscopy. The following features of interfaces are reviewed:the orientation relationships;the char- acteristic of steps,facets and ronghness of interfaces;atomic bonding across the interface;the degree of coherency,the structure of misfit dislocations and elastic relaxations at the inter- faces:the presence of defects at the onterfaces:the structure of the interfacial reaction prod- ucts as well as the reaction kinetics and reaetion mechanism.

关键词: fine structure of the interfaces , null , null , null

Structure and Mechanical Properties of High Si and Low C Steels

LIU Qingquan ZHANG Xiumu TENG Huayuan WANG Yikang Institute of Metal Research , Academia Sinica , Shenyang , 110015 , China

材料科学技术(英)

The investigation on lath martensitic transfor- mation has been carried out for 24SiMnNi2CrMoA steel using transmission electron microscopy (TEM) and X-ray diffraction.The austenite and martensite in the alloy adopt the intermediate orientation relationship between Kurdjumov-Sachs and Nishiyama.The adjacent laths in a packet are small-angle related or twin-related.The retained austenites which accommodate shape deformation of martensites appear commonly between adjacent laths.High Si content increases the volume fraction of retained austenites and its stability.The excellent combination of high strength and toughness of this steel is attributed to its fine martensite laths mingled with more than 5% continuous retained austenite films.

关键词: martensitic transformation , null , null , null

质子辐照A508-3钢显微组织和物相取向关系

丁辉 , 雷静 , 束国刚 , 万强茂

材料热处理学报

利用透射电镜研究了质子辐照对反应堆压力容器钢A508-3钢显微组织形态的影响,基于拍摄的铁素体与渗碳体的复合衍射花样,采用矩阵分析法研究了质子辐照前后试样铁素体与渗碳体之间的取向关系.结果表明,辐照前后A508-3钢的铁素体板条宽度和碳化物的尺寸、体积分数及分布没有发生明显变化.A508-3钢辐照至0.271 dpa时产生了分布较为均匀的位错环,位错环平均直径约为4.6 nm,数量密度约为2.7 ×1022m-3.在未辐照试样观察到铁素体和渗碳体的取向关系符合Bagaryatskii关系,而0.216 dpa和0.271 dpa辐照试样中观察到铁素体和渗碳体之间出现了3种新的取向关系.这3种新的取向关系的来源及对力学性能的影响值得深入研究.

关键词: 质子辐照 , 组织形态 , 矩阵分析法 , 取向关系

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